Chemical Synthesis Entity

id1
reactionIDR-0000-000001
Synthetic Scheme

reactant

reactantIDmoleculeIDimage
10230 N-0000-000001
10231 N-0000-000002
10232 N-0000-000003

reactant Detail

reactantID commentary mol volume weight number assigned by author
10230 1 equiv. 1alpha
10231 Yb(OTf)3 0.1 equiv.
10232 0.34 equiv. 2

product

productIDmoleculeIDimage
4004 N-0000-000004
4005 N-0000-000005

product Detail

productID commentary moleculeID image yield volume weight number assigned by author
4004 N-0000-000004 52% 3alpha
4005 by-product (boat) N-0000-000005 10%
4005 N-0000-000005 4alpha

reaction detail

reactionDetailID4480
reactionTime1.5 hours
reactionTemproom temp
solventCH2Cl2
ObjectTable 1/ Entry 1

reaction comment

reactionCommentIDcomment
4742 The PMID could not be found.
4743 Keywords: aryl O-glycoside, triaryloxyborane, ytterbium(III) trifluoromethanesulfonate

reaction references

reactionRefIDreferenceID
5749 REF-0000-000001

references

reactionRefID5749
referenceIDREF-0000-000001
sourceTetrahedron Letters 42 (2001) 4009-4011
doi10.1016/S0040-4039(01)00644-X

date

Registered2012 April 03, 07:47:20
Last Modified2013 August 16, 13:40:36